Modern Pharmaceutical Instrumental Analysis Techniques

Contents

The Course is based on Modern Pharmaceutical Analytical Techniques and covers the following topics in detail:

1. UV-Visible spectroscopy: Introduction, Theory, Laws, Instrumentation associated with UV-Visible spectroscopy, Choice of solvents and solvent effect and Applications of UV- Visible spectroscopy. b. IR spectroscopy: Theory, Modes of Molecular vibrations, Sample handling, Instrumentation of Dispersive and Fourier - Transform IR Spectrometer, Factors affecting vibrational frequencies and Applications of IR spectroscopy.

2. NMR spectroscopy: Quantum numbers and their role in NMR, Principle, Instrumentation, Solvent requirement in NMR, Relaxation process, NMR signals in various compounds, Chemical shift, Factors influencing chemical shift, Spin-Spin coupling, Coupling constant, Nuclear magnetic double resonance, Brief outline of principles of FT-NMR and 13C NMR. Applications of NMR spectroscopy.

3. Mass Spectroscopy: Principle, Theory, Instrumentation of Mass Spectroscopy, Different types of ionization like electron impact, Applications of Mass spectroscopy

4 . a) Electrophoresis: Principle, Instrumentation, Working conditions, factors affecting separation and applications of the following: a) Paper electrophoresis b) Gel electrophoresis c) Capillary electrophoresis d) Zone electrophoresis e) Moving boundary electrophoresis f) Iso electric focusing b) X ray Crystallography: Production of X rays, Different X ray diffraction methods, Bragg‘s law, Rotating crystal technique, X ray powder technique, Types of crystals and applications of Xray diffraction.

5. Thermal Techniques: Principle, thermal transitions and

Instrumentation (Heat flux and power-compensation and designs), Modulated DSC, Hyper DSC, experimental parameters (sample preparation, experimental conditions, calibration, heating and cooling rates, resolution, source of errors) and their influence, advantage and disadvantages, pharmaceutical applications.

Differential Thermal Analysis (DTA): Principle, instrumentation.

Note: For Instrumental Chromatographic Techniques , please attend the Chromatography Techniques Certificate Course of Ateos Foundation of Science Education and Research on Udemy Platform.

The course is exclusive creation of Ateos Foundation of Science Education and Research (AFSER) which is Non Profit Organization and holds statutory and mandatory requirements from Government of India , as well as Chartered under the Ministry of Corporate Affairs, Government of India. AFSER courses on Udemy platform awards, which is not individualized trainer certificates on this elegant platform for online Education. We wish the learners a very Happy Learning!!!